HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → Sodium 6-methoxynicotinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 6-methoxypyridine-3-carboxylate | HCID 586039 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Sodium 6-methoxynicotinate | HCID 23717611 | — |
Reaction Steps
methyl 6-methoxynicotinate (2.097 g, 12.56 mmol) was dissolved in dioxane (30 mL). An aqueous solution of NaOH (1.0N, 25 mL) was added to the solution and the mixture was stirred at room temperature overnight. The solvent was removed under reduced pressure to provide 2.2 g of sodium 6-methoxynicotinate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476399B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-e2d8fa50ed5c42fdb9b6db3e1b916b41 |
| Source note | uspto-grants-2009_01 |