HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indoline → HCID 178478370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indoline | HCID 10328 | — |
| Reactant | 2,6-Dichloropurine | HCID 5324412 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 178478370 | HCID 178478370 | 96.4% |
Reaction Steps
189 mg of 2,6-dichloropurine, 4 ml of butanol and 143 mg (1.2 equivalents) of indoline are mixed and brought to a temperature of 80° C. for approximately 17 hours. The mixture is allowed to return to ambient temperature. Partial drying, washing with ethyl ether and drying under vacuum are carried out, and 262 mg of expected product are obtained in the form of beige-colored crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476670B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-a44a95748b394c6c925860e1c8b6d536 |
| Source note | uspto-grants-2009_01 |