Sodium Iodide → HCID 178468895, compound

HRID 1453556Notes

Reaction equation

HRID 1453556 reaction equation
[N:1]1([C:10]2[N:18]=[C:17](Cl)[N:16]=[C:15]3[C:11]=2[N:12]=[CH:13][NH:14]3)[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[CH:2]1.[NH2:20][C:21]1[CH:22]=[C:23]([CH:29]=[CH:30][CH:31]=1)[C:24]([O:26][CH2:27][CH3:28])=[O:25].[Na+].[I-]>>[N:1]1([C:10]2[N:18]=[C:17]([NH:20][C:21]3[CH:22]=[C:23]([CH:29]=[CH:30][CH:31]=3)[C:24]([O:26][CH2:27][CH3:28])=[O:25])[N:16]=[C:15]3[C:11]=2[N:12]=[CH:13][NH:14]3)[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[CH:2]1

Participants

4

Reactant 3

HCID 5238Sodium IodideHCID 11400Ethyl 3-aminobenzoateHCID 178478376HCID 178478376, compound

Product 1

HCID 178468895HCID 178468895, compound

Conditions

Temperature
140 °C

Procedure

300 mg of product obtained in stage 1 above are mixed with 0.83 ml (5 equivalents) of ethyl 3-aminobenzoate and 0.166 mg of NaI, and the mixture is then heated at 140° C. for approximately 4 days.

Sources & evidence

ORD record
ord-19166511504543dca12f8946fc0f75db
Source dataset
uspto-grants-2009_01
Patent number
US07476670B2

Reaction notes

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