Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | HCID 178478376 | HCID 178478376 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 178419902 | HCID 178419902 | — |
Reaction Steps
200 mg of product obtained in stage 1 above are mixed with 2 ml of DMSO and 0.42 ml of cyclohexylamine, and the mixture is then heated at 110° C. for approximately 48 hours. The mixture is allowed to return to ambient temperature. Purification is carried out by chromatography on silica with a CH2Cl2-MeOH—NH4OH: 90-9-1 mixture for eluent. 84.7 mg of expected product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07476670B2 |
|---|
| Source dataset | uspto-grants-2009_01 |
|---|
| ORD ID | ord-0c349a75dd754630bd30f2f39de27332 |
|---|
| Source note | uspto-grants-2009_01 |
|---|
