HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1453590Generated: October 30, 2026
2-Amino-1-butanol → HCID 178456044, compound
https://huagongshe.com/reaction/1453590
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Amino-1-butanol | HCID 22129 | — |
| Reactant | HCID 178478376 | HCID 178478376 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 178456044 | HCID 178456044 | — |
Reaction Steps
200 mg of product obtained in stage 1 above are mixed with 3 ml of DMSO and 350 μl (5 equivalents) of (+/−)-2-amino-1-butanol, and the mixture is then heated at 120° C. for approximately 2 days. The mixture is allowed to return to ambient temperature. Purification is carried out by chromatography on silica with a CH2Cl2-MeOH—NH4OH: 95-5-0.3 mixture for eluent. 40 mg of expected product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07476670B2 |
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| Source dataset | uspto-grants-2009_01 |
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| ORD ID | ord-6030d3a0525f4a798c18001d492b4394 |
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| Source note | uspto-grants-2009_01 |
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