HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1453594Generated: October 30, 2026
HCID 178421931, compound → HCID 178421930, compound
https://huagongshe.com/reaction/1453594
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 178421931 | HCID 178421931 | — |
| Reactant | HCID 178511674 | HCID 178511674 | — |
| Product | HCID 178421930 | HCID 178421930 | 24.1% |
Reaction Steps
The same procedure as in stage 2 of Example 1 is carried out, starting from 684 mg of trans-1,4-diaminocyclohexane and 166 mg of the product obtained in stage 2 above, and the mixture is heated at 140° C. for 6 hours. Purification is carried out on silica with MeOH—NH4OH: 98-2 for eluent, and 51 mg of expected product are thus obtained, in the form of beige-colored crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07476670B2 |
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| Source dataset | uspto-grants-2009_01 |
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| ORD ID | ord-7f5ec8513257427ea38a86e372add63b |
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| Source note | uspto-grants-2009_01 |
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