HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178525679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Anisole | HCID 7519 | — |
| Reactant | HCID 178451976 | HCID 178451976 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178525679 | HCID 178525679 | — |
Reaction Steps
35 mg of the product of Example 31 are mixed with 1 ml of CH2Cl2 and 0.5 ml of TFA containing 10% of anisole. The mixture is left to stir for 2 hours at ambient temperature, followed by concentrating to dryness in the presence of toluene and of CH2Cl2. 40 mg of expected product are thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476670B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-88aa826fd34049f5a8e425426af98aa2 |
| Source note | uspto-grants-2009_01 |