HRID1453603
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
35 mg of the product of Example 31 are mixed with 1 ml of CH2Cl2 and 0.5 ml of TFA containing 10% of anisole. The mixture is left to stir for 2 hours at ambient temperature, followed by concentrating to dryness in the presence of toluene and of CH2Cl2. 40 mg of expected product are thus obtained.
WORKUP
后处理
- waitThe mixture is left
- concentrationby concentrating to dryness in the presence of toluene and of CH2Cl2