HRID1453603

反应详情

EQUATION

反应方程式

HRID 1453603 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

35 mg of the product of Example 31 are mixed with 1 ml of CH2Cl2 and 0.5 ml of TFA containing 10% of anisole. The mixture is left to stir for 2 hours at ambient temperature, followed by concentrating to dryness in the presence of toluene and of CH2Cl2. 40 mg of expected product are thus obtained.

WORKUP

后处理

  1. waitThe mixture is left
  2. concentrationby concentrating to dryness in the presence of toluene and of CH2Cl2