HCID 178511674, compound → HCID 178465944, compound

Participants

Reaction Conditions

Reaction Steps

1.88 g of product obtained in stage 1 above are mixed with 4.8 g of trans-1,4-diaminocyclohexane, and the mixture is then heated at 140° C. for approximately 72 hours. The mixture is allowed to return to ambient temperature for 48 hours. A paste is formed in water, and drying is carried out under vacuum at 50° C. 2.7 g of expected product are obtained, in the form of a beige powder.

Provenance & Evidence