HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Nitroindoline → HCID 178526437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Nitroindoline | HCID 36219 | — |
| Reactant | 2,6-Dichloropurine | HCID 5324412 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 178526437 | HCID 178526437 | 90.6% |
Reaction Steps
37.8 g of 2,6-dichloropurine, 700 ml of butanol and 32.8 g of 5-nitroindoline are mixed and brought to a temperature of 90° C. for approximately 3 days. The mixture is allowed to return to ambient temperature. Partial drying, washing with ethyl ether and drying under vacuum at 50° C. are carried out and 57.3 g of expected product are obtained, in the form of beige crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476670B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-d320f36f5fa9491a829b26543dd63f07 |
| Source note | uspto-grants-2009_01 |