HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 178454026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 2-Thiopheneacetyl chloride | HCID 162362 | — |
| Reactant | HCID 178454025 | HCID 178454025 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178454026 | HCID 178454026 | — |
Reaction Steps
40 mg of product obtained in stage 4 are mixed with 11.4 mg of 2-thiopheneacetyl chloride, 25 μl of diisopropylethylamine and 2 ml of dichloromethane. The mixture is stirred for 1 hour at ambient temperature, and then washing with brine, drying over magnesium sulfate and evaporation to dryness are carried out.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476670B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-9f4bbec9b5274006bc6dace5f08619b4 |
| Source note | uspto-grants-2009_01 |