HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Methyl-4-nitrophenyl)-1,4-oxazepan-5-one → 3-Methyl-4-(5-oxo-[1,4]oxazepan-4-yl)-aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Methyl-4-nitrophenyl)-1,4-oxazepan-5-one | HCID 59586730 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Methyl-4-(5-oxo-[1,4]oxazepan-4-yl)-aniline | HCID 59586774 | — |
Reaction Steps
Prepared analogously to Example 1c from 3-methyl-4-(5-oxo-[1,4]oxazepan-4-yl)-1-nitro-benzene with Raney nickel under a hydrogen atmosphere in methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476663B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-fb5b4ff9ab614ce2b0f5f4d23cb8663f |
| Source note | uspto-grants-2009_01 |