Potassium tertbutoxide → HCID 69052229, compound

HRID 1453664Notes

Reaction equation

HRID 1453664 reaction equation

[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[NH:11][C:12](=[O:19])[O:13][CH2:14][CH2:15][CH2:16][CH2:17]Cl.[K].CC(C)([O-])C>CN(C=O)C>[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]1[CH2:17][CH2:16][CH2:15][CH2:14][O:13][C:12]1=[O:19]

Participants

4

Reactant 2

HCID 50987170Potassium tertbutoxide

HCID 69054781HCID 69054781, compound

Product 1

HCID 69052229HCID 69052229, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared analogously to Example 39b from 4-chloro-butyl 2-methyl-4-nitro-phenyl-carbamate with potassium-tert.-butoxide in DMF.

Sources & evidence

ORD record: ord-e3baae65cd124a7593428a4be792dda8
Source dataset: uspto-grants-2009_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07476663B2

Reaction notes

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