HCID 69052229, compound → HCID 69057404, compound

HRID 1453665Notes

Reaction equation

HRID 1453665 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([N+:16]([O-])=O)[CH:5]=[CH:6][C:7]=1[N:8]1[CH2:14][CH2:13][CH2:12][CH2:11][O:10][C:9]1=[O:15]>C1COCC1.[Pd]>[CH3:1][C:2]1[CH:3]=[C:4]([CH:5]=[CH:6][C:7]=1[N:8]1[CH2:14][CH2:13][CH2:12][CH2:11][O:10][C:9]1=[O:15])[NH2:16]

Participants

4

Reactant 1

HCID 69052229HCID 69052229, compound

Product 1

HCID 69057404HCID 69057404, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 8028TetrahydrofuranSolvent

Procedure

Prepared analogously to Example 40b from 3-methyl-4-(2-oxo-[1,3]oxazepan-3-yl)-1-nitro-benzene with palladium-charcoal under a hydrogen atmosphere in THF.

Sources & evidence

ORD record
ord-b8b59e032191442f95d0445c13aa6d24
Source dataset
uspto-grants-2009_01
Patent number
US07476663B2

Reaction notes

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