HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 64888821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-Bromothiophene-2-carboxylic acid | HCID 349115 | — |
| Reactant | 3-Aminotetrahydrofuran-3-carboxylic acid | HCID 543662 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 64888821 | HCID 64888821 | — |
Reaction Steps
Prepared analogously to Example 53a from 3-amino-tetrahydrofuran-3-carboxylic acid and 5-bromo-thiophene-2-carboxylic acid with thionyl chloride and N,O-bis-(trimethylsilyl)-trifluoroacetamid in dichloromethane with triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476663B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-5aad11ab4c9d459f8e4df41dce459861 |
| Source note | uspto-grants-2009_01 |