Sodium Hydroxide → HCID 46890685, compound

Participants

Reaction Conditions

Reaction Steps

The product from step c) (100 mg) was dissolved in 3 mL EtOH and treated with 0.5 mL of 1 M NaOH. The reaction was heated to 50° C. for 2 h. Upon cooling, the reaction was washed with DCM, acidified with 1 M HCl, and extracted into DCM. The organic layer was washed twice with water, dried over MgSO4, and concentrated to give the title compound as a solid. MS: ESI (negative): 375, 377 (M−H).

Provenance & Evidence