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HRID1453704

反应详情

EQUATION

反应方程式

HRID 1453704 的结构方程式

REACTANTS

反应物

2
结构：OCCBr
HCID10898

2-Bromo-1-ethanol

C2H5BrO

结构：Cc1c(C2NS(=O)(=O)c3ccccc32)c2ccccc2n1CC(=O)OC(C)(C)C
HCID67317115

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(C2c3ccccc3S(=O)(=O)N2CCO)c2ccccc2n1CC(=O)O
HCID46890209

未命名化合物

PROCEDURE

实验过程

The title compound was prepared by the method described for example 14 using the product from example 3, step c) and 2-bromoethanol. 1H NMR (DMSO-d6) δ 7.98-7.95 (m, 1H), 7.62-7.58 (m, 3H), 7.36 (d, J=8.4 Hz, 1H), 7.04-7.01 (m, 2H), 6.80-6.78 (m, 1H), 6.14 (s, 1H), 5.00 (s, 2H), 4.75 (bs, 1H), 3.59-3.53 (m, 1H), 3.26-3.17 (m, 2H), 3.02-2.92 (m, 1H), 2.39 (s, 3H); MS: ESI (negative): 399 (M−H).