HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 934282-57-2
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | (R)-5-(3-chlorophenyl)-3-(1-((4-Methyl-5-(pyridin-4-yl)-4H-1,2,4-triazol-3-yl)oxy)ethyl)isoxazole | HCID 16041426 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 934282-57-2 | HCID 69007598 | — |
Reaction Steps
An oiled salt was manufactured by evaporating a clear solution obtained by mixing 500 μl water with 33 mg 4-(5-{(1R)-1-[5-(3-chlorophenyl)isoxazol-3-yl]ethoxy}-4-methyl-4H-1,2,4-triazol-3-yl)pyridine free base, 500 μl methanol and 7 μl 98 wt-% sulphuric acid. The title salt was manufactured by recrystallising the oiled salt in 500 μl ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476684B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-83a06e85bf604f8b98d16bc6fcbaad09 |
| Source note | uspto-grants-2009_01 |