HRID1453953

反应详情

EQUATION

反应方程式

HRID 1453953 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

tert-butyl 4-[1-(2,4-dimethoxybenzyl)-2-oxo-1,4-dihydropyrido[3,2-d]pyrimidin-3(2H)-yl]piperidine-1-carboxylate (0.10 g, 0.21 mmol) was dissolved in trifluoroacetic acid (5 mL) and stirred overnight. The reaction concentrated to afford the bisTFA salt of the title compound (0.048 g). MS 233.2 (M+1).

WORKUP

后处理

  1. concentrationThe reaction concentrated