HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86605571, compound → 844503-06-6
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86605571 | HCID 86605571 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 844503-06-6 | HCID 54105929 | 90.7% |
Reaction Steps
A solution of 3-(2-azidoethyl)-2-nitropyridine (0.190 g, 0.98 mmol) in methanol (5 mL) was stirred at 20° C. with 10% palladium on carbon (50 mg) under 1 atm hydrogen for 96 h. The mixture was filtered through celite and the filtrate concentrated to give the title compound (0.122 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07476665B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-9c891b052f434b9886484b683474ae87 |
| Source note | uspto-grants-2009_01 |