HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl-5-bromo-2-carboxypyridine → 1-(5-Bromopyridin-2-yl)cyclopentan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl-5-bromo-2-carboxypyridine | HCID 67144082 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-(5-Bromopyridin-2-yl)cyclopentan-1-ol | HCID 69060998 | — |
Reaction Steps
The title compound was prepared using ethyl-5-bromo-2-carboxypyridine, 1,4-bis (bromomagnesium) butane and diethyl ether as solvent, but otherwise followed the general procedure for Preparation 36. 13C NMR (100 MHz, CDCl3) d 164.1, 148.9, 139.5, 120.9, 118.8, 83.2, 42.7, 24.9; MS (AP/Cl) 242.1, 244.1 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07479559B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-11c64e62e8c84a3e82c21855e36b08a1 |
| Source note | uspto-grants-2009_01 |