HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonamide → HCID 86607707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonamide | HCID 7370 | — |
| Reactant | 3-bromo-N-butyl-5-formyl-4-methoxy-benzenesulfonamide | HCID 86607708 | — |
| Product | HCID 86607707 | HCID 86607707 | 178.3% |
Reaction Steps
Proceeding as in Reference 19, but substituting 3-bromo-N-butyl-5-formyl-4-methoxy-benzenesulfonamide (0.65 g, 1.72 mmol) and N-tert-butyl-3-4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)benzenesulfonamide (0.64 g, 1.90 mmol, 1.1 eq.), gave N-butyl-N′-tert-butyl-5-formyl-6-methoxy-biphenyl-3,3′-disulfonamide (0.74 g) as on orange oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07479502B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-3bfc1b0076cf477b8753c98ea1cb10f4 |
| Source note | uspto-grants-2009_01 |