1-(4-Morpholinophenyl)-1-phenylprop-2-yn-1-ol → 3-phenyl-3-(4-morpholinophenyl)-13,13-dimethyl-3H,13H-indeno[2',3':3,4]naphtho[1,2-b]pyran

Participants

Reaction Steps

The process for Step 3 of Example 1 was followed except that 1-(4-morpholinophenyl)-1-phenyl-2-propyn-1-ol (from Step 2) was used instead of 1-ferrocenyl-1-phenyl-2-propyn-1-ol to react with 7,7-dimethyl-7H-benzo[C]fluoren-5-ol to provide 3-phenyl-3-(4-morpholinophenyl)-13,13-dimethyl-3H,13H-indeno[2′,3′:3,4]naphtho[1,2-b]pyran. Mass spectrometry analysis supported a molecular weight consistent with 3-phenyl-3-(4-morpholinophenyl)-13,13-dimethyl-3H,13H-indeno[2′,3′:3,4]naphtho[1,2-b]pyran.

Provenance & Evidence