HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86620812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triphenylsulfonium chloride | HCID 61343 | — |
| Reactant | Potassium | HCID 5462222 | — |
| Reactant | HCID 86620813 | HCID 86620813 | — |
| Product | HCID 86620812 | HCID 86620812 | 79% |
Reaction Steps
COMP CD-8 was prepared similar to COMP CD-7 at 79% yield from potassium salt of 3-oxo-2-cyanopropanoic acid t-butyl ester (2.07 g, 10 mmol) and 50% solution of triphenylsulfonium chloride in water (5.96 g, 10 mmol) as a yellow color, light weight (fluffy) crystalline material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482113B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-038bffab496c45838222c722c8aba08d |
| Source note | uspto-grants-2009_01 |