HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → 51519-09-6
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | Aminopyrazine | HCID 78747 | — |
| Product | 51519-09-6 | HCID 12229475 | — |
Reaction Steps
A solution of 2-aminopyrazine (16.45 g) in dimethylformamide dimethylacetal (22.4 g) was refluxed at 85° C. for 3 h, evaporated under reduced pressure, and used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482336B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-f0e41c090fba493da97c1f7fcb804e13 |
| Source note | uspto-grants-2009_01 |