HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → N-(5-Hydroxymethyl-6-methyl-pyridin-2-yl)-2,2-dimethyl-propionamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | N-(5-Formyl-6-methyl-pyridin-2-yl)-2,2-dimethyl-propionamide | HCID 86233848 | — |
| Product | N-(5-Hydroxymethyl-6-methyl-pyridin-2-yl)-2,2-dimethyl-propionamide | HCID 68844472 | — |
Reaction Steps
This material was prepared in analogy to example 107 step B] from N-(5-formyl-6-methyl-pyridin-2-yl)-2,2-dimethyl-propionamide (5.9 g) and sodium borohydride (1.037 g) as a light yellow solid (1.41 g). MS (ESI): 223.2 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-52bf7552bd1a410190dda7ea9a0d3bfd |
| Source note | uspto-grants-2009_01 |