HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Fluoro-2-methylbenzenesulphonyl chloride → N-(5-Cyclopropylmethoxymethyl-6-methyl-pyridin-2-yl)-5-fluoro-2-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Fluoro-2-methylbenzenesulphonyl chloride | HCID 136286 | — |
| Reactant | 5-Cyclopropylmethoxymethyl-6-methyl-pyridin-2-ylamine | HCID 68843148 | — |
| Product | N-(5-Cyclopropylmethoxymethyl-6-methyl-pyridin-2-yl)-5-fluoro-2-methyl-benzenesulfonamide | HCID 68845292 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 5-cyclopropylmethoxymethyl-6-methyl-pyridin-2-ylamine (0.053 g) and 5-fluoro-2-methyl-benzenesulfonyl chloride (0.058 g) as a light yellow solid (0.063 g). MS (ESI−): 363.3 ([M−H]−)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-f7377151274341ca8bc8ceb5d6213a39 |
| Source note | uspto-grants-2009_01 |