HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → 3-Chloro-N-(5-ethoxymethyl-6-methyl-pyridin-2-yl)-2-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 5-Ethoxymethyl-6-methyl-pyridin-2-ylamine | HCID 68840827 | — |
| Product | 3-Chloro-N-(5-ethoxymethyl-6-methyl-pyridin-2-yl)-2-methyl-benzenesulfonamide | HCID 68846568 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 5-ethoxymethyl-6-methyl-pyridin-2-ylamine (0.066 g) and 3-chloro-2-methyl-benzenesulfonyl chloride (0.099 g) as an off-white solid (0.08 g). MS (ESI−): 351.3 ([M−H]−)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-8d9a06fcc4ab4cbab731ddc2cda6a67b |
| Source note | uspto-grants-2009_01 |