HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorotoluene-2-sulphonyl chloride → 3-Chloro-N-(5-cyclopropylmethoxymethyl-6-methyl-pyridin-2-yl)-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorotoluene-2-sulphonyl chloride | HCID 100415 | — |
| Reactant | 5-Cyclopropylmethoxymethyl-6-methyl-pyridin-2-ylamine | HCID 68843148 | — |
| Product | 3-Chloro-N-(5-cyclopropylmethoxymethyl-6-methyl-pyridin-2-yl)-benzenesulfonamide | HCID 68845407 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 5-cyclopropylmethoxymethyl-6-methyl-pyridin-2-ylamine (0.06 g) and 3-chloro-6-methyl-benzenesulfonyl chloride (0.072 g) as a light yellow solid (0.07 g). MS (ESI−): 364.9 ([M−H] )
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-69a002eec6eb43dc98307967bd4656e6 |
| Source note | uspto-grants-2009_01 |