HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-methylbenzenesulfonyl chloride → 2,4-Dichloro-N-(5-cyclopropylmethoxymethyl-6-methyl-pyridin-2-yl)-6-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| Reactant | 5-Cyclopropylmethoxymethyl-6-methyl-pyridin-2-ylamine | HCID 68843148 | — |
| Product | 2,4-Dichloro-N-(5-cyclopropylmethoxymethyl-6-methyl-pyridin-2-yl)-6-methyl-benzenesulfonamide | HCID 68842935 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 5-cyclopropylmethoxymethyl-6-methyl-pyridin-2-ylamine (0.06 g) and 2,4-dichloro-6-methyl-benzenesulfonyl chloride (0.089 g) as an amorphous light yellow solid (0.058 g). MS (ESI−): 413.1 ([M−H]−)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-439b194095df42b196f6c3554bd664f8 |
| Source note | uspto-grants-2009_01 |