HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-methylbenzenesulfonyl chloride → 2,4-Dichloro-N-[6-(3-fluoro-benzyloxymethyl)-pyridin-2-yl]-6-methyl-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| Reactant | 6-(3-Fluoro-benzyloxymethyl)-pyridin-2-ylamine | HCID 68840781 | — |
| Product | 2,4-Dichloro-N-[6-(3-fluoro-benzyloxymethyl)-pyridin-2-yl]-6-methyl-benzenesulfonamide | HCID 68842604 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 6-(3-fluoro-benzyloxymethyl)-pyridin-2-ylamine (0.06 g) and 2,4-dichloro-6methyl-benzenesulfonyl chloride (0.074 g) as a yellow solid (0.12 g). MS (ESI−): 453.1 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-01c932ca51a44c4bbe917c8a24b0e415 |
| Source note | uspto-grants-2009_01 |