HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chlorobenzenesulphonyl chloride → 3-Chloro-N-[6-(2-cyclopropyl-ethoxymethyl)-pyridin-2-yl]-benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chlorobenzenesulphonyl chloride | HCID 17909 | — |
| Reactant | 6-(2-Cyclopropyl-ethoxymethyl)-pyridin-2-ylamine | HCID 68842176 | — |
| Product | 3-Chloro-N-[6-(2-cyclopropyl-ethoxymethyl)-pyridin-2-yl]-benzenesulfonamide | HCID 68842964 | — |
Reaction Steps
This material was prepared in analogy to example 1 from 6-(2-cyclopropyl-ethoxymethyl)-pyridin-2-ylamine (0.08 g) and 3-chloro-benzenesulfonyl chloride (0.095 g) as a light yellow gum (0.096 g). MS (ESI−): 365.0 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-9a37aeeb21f5453496572a723155bffe |
| Source note | uspto-grants-2009_01 |