HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → HCID 68842087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 5-Phenoxypyridin-2-amine | HCID 22179454 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 68842087 | HCID 68842087 | 18.4% |
Reaction Steps
5-Phenoxy-pyridin-2-ylamine (100 mg) was treated with 3-chloro-2-methylbenzenesulfonyl chloride (122 mg) in the presence of pyridine (3 mL) as described in example 172, step C] to give 3-Chloro-2-methyl-N-(5-phenoxy-pyridin-2-yl)-benzenesulfonamide (37 mg) as a white foam. MS (ESI): 375.1 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482341B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-8433362758354f2dae96de221fa80453 |
| Source note | uspto-grants-2009_01 |