N-Phenyl-p-phenylenediamine → HCID 12106063, compound

HRID 1454926Notes

Reaction equation

[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]([C:10]([OH:12])=O)=[N:2]1.[C:13]1([NH:19][C:20]2[CH:25]=[CH:24][C:23]([NH2:26])=[CH:22][CH:21]=2)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.C1(N=C=NC2CCCCC2)CCCCC1>>[C:13]1([NH:19][C:20]2[CH:25]=[CH:24][C:23]([NH:26][C:10]([C:3]3[C:4]4[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=4)[NH:1][N:2]=3)=[O:12])=[CH:22][CH:21]=2)[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1

Participants

Reactant 3

HCID 7564N-Phenyl-p-phenylenediamine

HCID 10868Dicyclohexylcarbodiimide

HCID 78250Indazole-3-carboxylic acid

Product 1

HCID 12106063HCID 12106063, compound

Procedure

This compound is synthesized in a manner similar to the procedure described in Example 2 by coupling indazole-3-carboxylic acid and N-phenyl-1,4-phenylenediamine on the scale of 1 mmol, but using dicyclohexylcarbodiimide (DCC) as coupling reagent. The crude product obtained after extraction is taken up in CHCl3. The insoluble matter is filtered and dried.

Workup

customThis compound is synthesized in a manner similar to the procedure

Sources & evidence

ORD record: ord-caa7aded33c64971879085806f129b98
Source dataset: uspto-grants-2009_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07482342B2

Reaction notes

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