HuagongsheHuagongshe Chemistry Print Report · For research reference only
Selectfluor → HCID 178461800, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Selectfluor | HCID 2724933 | — |
| Reactant | HCID 178461795 | HCID 178461795 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178461800 | HCID 178461800 | — |
Reaction Steps
The product of Example 3 (0.1 g) was dissolved in methanol (10 ml), Selectfluor™ (0.12 g) added and stirred for 20 h. The mixture was evaporated and purified by silica gel chromatography (5% methanol/DCM) to yield the title product as a white solid. Yield 19 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482355B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-4f821785523a439abb537ba1059fa179 |
| Source note | uspto-grants-2009_01 |