HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 22392771, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Benzeneacetic acid, 4-hydroxy-, methyl ester | HCID 518900 | — |
| Reactant | 4-(Chloromethyl)-2-methylquinoline | HCID 11535719 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 22392771 | HCID 22392771 | — |
Reaction Steps
To a solution of methyl (4-hydroxyphenyl)acetate (10.0 g, 60.2 mmol) in 400 mL THF was added 4-chloromethyl-2-methylquinoline (11.5 g, 60.2 mmol), cesium carbonate (29.4 g, 90.3 mmol), and sodium iodide (451 mg, 3 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482372B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-73034c943c784995a14c91ce85cd2ecf |
| Source note | uspto-grants-2009_01 |