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HRID1455561

反应详情

EQUATION

反应方程式

HRID 1455561 的结构方程式

REACTANTS

反应物

2
结构：N
HCID222

Ammonia gas

H3N

结构：O=S(=O)(Cl)c1cc(C(F)(F)F)cc(C(F)(F)F)c1
HCID520945

3,5-Bis(trifluoromethyl)benzenesulphonyl chloride

C8H3ClF6O2S

PRODUCTS

生成物

1
结构：NS(=O)(=O)c1cc(C(F)(F)F)cc(C(F)(F)F)c1
HCID2783165

3,5-bis(trifluoromethyl)benzenesulfonamide

C8H5F6NO2S

PROCEDURE

实验过程

An aqueous solution of NH3 (32%) is added at room temperature to a solution of 3,5-bis-(trifluoromethyl)benzene-sulfonylchloride in EtAc. The mixture obtained is stirred and two phases obtained are separated, the organic layer obtained is washed with 1 N HCl and H2O, and dried. Solvent of the organic solution obtained is evaporated. 3,5-Bis-trifluoromethyl-benzene sulfonamide is obtained.

WORKUP

后处理

  1. customThe mixture obtained
  2. customtwo phases obtained
  3. customare separated
  4. customthe organic layer obtained
  5. washis washed with 1 N HCl and H2O
  6. customdried
  7. customSolvent of the organic solution obtained
  8. customis evaporated