3,5-Dibromopyridine → HCID 68956246, compound

HRID 1455631Notes

Reaction equation

HRID 1455631 reaction equation
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6](B(O)O)=[CH:5][CH:4]=1.[Br:12][C:13]1[CH:14]=[N:15][CH:16]=[C:17](Br)[CH:18]=1>CCOC(C)=O>[Br:12][C:13]1[CH:14]=[N:15][CH:16]=[C:17]([C:6]2[CH:7]=[CH:8][C:3]([S:2][CH3:1])=[CH:4][CH:5]=2)[CH:18]=1

Participants

4

Reactant 2

HCID 693693,5-DibromopyridineHCID 27339594-(Methylthio)phenylboronic acid

Product 1

HCID 68956246HCID 68956246, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

Prepared according to the procedure Coupling-2 using [4-(methylthio)phenyl]boronic acid and 3,5-dibromopyridine as starting material. Flash chromatography (Hex:EtOAc; 95:5-85:15) afforded the title compound

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-9c006cfccac844878cea559db7517cde
Source dataset
uspto-grants-2009_01
Patent number
US07482456B2

Reaction notes

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