HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 178434719, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 178434729 | HCID 178434729 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 178434719 | HCID 178434719 | — |
Reaction Steps
A solution 3-(3-methyl-1,2,4-oxadiazol-5-yl)pyridin-2-ol in AcOH (0.2M) and bromine (1.2 eq) was stirred 18 h at 20° C. and then concentrated. The residue was co-evaporated with benzene (2×) and used as such in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482456B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-9cefcca1589d4fd697cb14e0d74e8f2b |
| Source note | uspto-grants-2009_01 |