Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 178434719 | HCID 178434719 | — |
| Catalyst | HCID 178418647 | HCID 178418647 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 57535395 | HCID 57535395 | — |
Reaction Steps
A solution 5-bromo-3-(3-methyl-1,2,4-oxadiazol-5-yl)pyridin-2-ol (1 eq) in benzene (0.05M) was added silver carbonate (1 eq) and benzyl bromide (1.2 eq). The reaction mixture was stirred 6 h at 20° C. and then concentrated. The residue was purified by flash chromatography (Hexane:EtOAc, 90:10) to afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07482456B2 |
|---|
| Source dataset | uspto-grants-2009_01 |
|---|
| ORD ID | ord-e0e9635af48947528f6c3d1adbf315fb |
|---|
| Source note | uspto-grants-2009_01 |
|---|
