3-Bromothiophene → HCID 54448499, compound

HRID 1455645Notes

Reaction equation

HRID 1455645 reaction equation
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6](B(O)O)=[CH:5][CH:4]=1.Br[C:13]1[CH:17]=[CH:16][S:15][CH:14]=1>C(Cl)Cl>[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([C:13]2[CH:17]=[CH:16][S:15][CH:14]=2)=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 133833-BromothiopheneHCID 27339594-(Methylthio)phenylboronic acid

Product 1

HCID 54448499HCID 54448499, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Prepared according to the procedure Coupling-1 using [4-(methylthio)phenyl]boronic acid and 3-bromothiophene as starting material. Flash chromatography (CH2Cl2) afforded the title compound.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-4b9023e8b60a4f2bacef9200c7307092
Source dataset
uspto-grants-2009_01
Patent number
US07482456B2

Reaction notes

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