HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dibromobenzene → 4-(3-Bromophenyl)pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dibromobenzene | HCID 7927 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | (Pyridin-4-yl)boronic acid | HCID 2734379 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(3-Bromophenyl)pyridine | HCID 13150402 | — |
Reaction Steps
Prepared according to the general procedure Coupling-1 using 4-pyridinylboronic acid and 1,3-dibromobenzene. Flash chromatography (Hexane:EtOAc, 70:30) afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482456B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-11777189074d4987b67e942c04f208c1 |
| Source note | uspto-grants-2009_01 |