1,2-Dibromobenzene → HCID 23436728, compound

HRID 1455656Notes

Reaction equation

HRID 1455656 reaction equation
[C:1]([C:4]1[CH:9]=[CH:8][C:7](B(O)O)=[CH:6][CH:5]=1)(=[O:3])[CH3:2].[Br:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1Br>CCOC(C)=O>[Br:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[C:7]1[CH:8]=[CH:9][C:4]([C:1](=[O:3])[CH3:2])=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 114141,2-DibromobenzeneHCID 37021224-Acetylphenylboronic acid

Product 1

HCID 23436728HCID 23436728, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

Prepared according to the general procedure Coupling-1 using 4-acetylbenzeneboronic acid and 1,2-dibromobenzene as starting material. Flash chromatography (Hex:EtOAc; 95:5) afforded the title compound.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-fc3981ec3ed249ff8b1e55540e94f72e
Source dataset
uspto-grants-2009_01
Patent number
US07482456B2

Reaction notes

Loading…