HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 9991546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 12144845 | HCID 12144845 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 9991546 | HCID 9991546 | — |
Reaction Steps
5.6 g (22.7 mmol) of 5-hexyl-6-methoxyindan-1-one, 9.4 g of aluminium chloride and 125 ml of toluene are refluxed for 15 minutes. The mixture is poured into water and extracted with ether. The organic phase is dried (Na2SO4) and the solvents are evaporated off. The residue is purified by flash chromatography (4.5 g; 85%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482484B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-2002783d70f54fcf8b8cee99f7fa332c |
| Source note | uspto-grants-2009_01 |