HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 9992783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 10423493 | HCID 10423493 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 9992783 | HCID 9992783 | — |
Reaction Steps
1.93 g (7 mmol) of 5-hexyl-6-methoxy-2,2-dimethylindan-1-one, 2.84 g (21 mmol) of aluminium chloride and 40 ml of toluene are heated for 15 minutes at reflux. The mixture is poured into water and extracted with ether. The organic phase is dried (Na2SO4) and the solvent evaporated off. The residue is purified by flash chromatography (dichloromethane, 2.8 g; 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07482484B2 |
| Source dataset | uspto-grants-2009_01 |
| ORD ID | ord-894103825a6c4380be4d9a8b386e4cee |
| Source note | uspto-grants-2009_01 |