HRID1455704

反应详情

EQUATION

反应方程式

HRID 1455704 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 6-hydroxy-5-iodoindan-1-one (6.36 g, 23.2 mmol), caesium carbonate (15.12 g, 46.4 mmol) and ethyl4-bromobutyrate (9.05 g, 46.4 mmol) in acetone (60 ml) is heated at reflux pendant 1 hour 15 minutes.

WORKUP

后处理

  1. temperatureis heated
  2. temperatureat reflux pendant 1 hour 15 minutes