Diethyl Ether → HCID 22105525, compound

Participants

Reaction Steps

tert-Butyl-4-[N-(2-benzyloxybenzyl)-N-ethylamino]-2-fluorobenzoate (1.81 g) in formic acid (5 mL) was heated on a steam bath until a clear solution was obtained. The reaction mixture was evaporated to dryness and the oil obtained solidified on trituration with diethyl ether to give 4-[N-(2-benzyloxybenzyl)-N-ethylamino]-2-fluorobenzoic acid, yield 0.51 g, mp 154° C.

Provenance & Evidence