Ethyl Acetate → 1-[5-(2-Methoxyethyl)-4-methyl-2-thiazolyl]ethanone

HRID 1456331Notes

Reaction equation

[CH3:1][O:2][CH2:3][CH2:4][C:5]1[S:9][CH:8]=[N:7][C:6]=1[CH3:10].[C:11](OCC)(=[O:13])[CH3:12]>>[C:11]([C:8]1[S:9][C:5]([CH2:4][CH2:3][O:2][CH3:1])=[C:6]([CH3:10])[N:7]=1)(=[O:13])[CH3:12]

Participants

Reactant 2

HCID 8857Ethyl Acetate

HCID 11159460HCID 11159460, compound

Product 1

HCID 221066951-[5-(2-Methoxyethyl)-4-methyl-2-thiazolyl]ethanone

Procedure

From 5-(2-methoxyethyl)-4-methylthiazole and ethyl acetate, following the procedure of Preparation 1. 13C Nmr (CDCl3) 15.1, 25.6, 27.6, 58.7, 71.9, 137.9, 151.6, 163.0 and 191.5 ppm.

Workup

customthe procedure of Preparation 1

Sources & evidence

ORD record: ord-b8f2f662413a44d59f0518e55825dfaa
Source dataset: uspto-grants-1998_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05843971

Reaction notes

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