HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromothiazole → HCID 9860114, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromothiazole | HCID 76430 | — |
| Reactant | 2,2,2-Trifluoro-1-(1,3-thiazol-2-yl)ethan-1-one | HCID 22106684 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 9860114 | HCID 9860114 | — |
Reaction Steps
From 2-bromothiazole and 2-trifluoroacetylthiazole. M.p. 113°-115° C. 13C Nmr (d6 -DMSO) 77.3 (q, J 30Hz), 122.8, 123.0 (q, J 286 Hz), 142.7 and 166.1 ppm. Found: C, 36.25; H, 1.7; N, 10.5. C8H5F3N2OS2 requires C, 36.1; H, 1.9; N, 10.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05843971 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-b8441b37972741b69adf9e16fff4750d |
| Source note | uspto-grants-1998_12 |