HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22915156, compound → HCID 54000870, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22915156 | HCID 22915156 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54000870 | HCID 54000870 | — |
Reaction Steps
The product from Example 19 in ethanol was hydrogenated in the presence of 10% palladium-on-charcoal to give the title compound. 1H Nmr (CDCl3) 2.02, 2.08 and 2.61 (each 3H, s), 2.23 (2H, br s) and 7.28 and 7.73 (each 1H, d, J 3 Hz) ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05843971 |
| Source dataset | uspto-grants-1998_12 |
| ORD ID | ord-127e73afd7df4687a6971bd5286e5854 |
| Source note | uspto-grants-1998_12 |